Thermo Orbitrap have the best Resolving power: 70,000 at m/z 200. Q Exactive GC Manuals - English. Conventions Within this manual, the following conventions are used: WARNING!
The Q Exactive Focus MS offers quantitative analyses at up to 6 orders of magnitude of linear quantitative dynamic range. Quanfirmation Plus — Characterize, Quantify & Confirm. This guide is intended for all personnel who operate the Q Exactive Plus mass spectrometer.
APCI Ion Source Manual About This Manual 1 About This Manual This manual contains the instructions required to operate the atmospheric pressure chemical ionization (APCI) ion source (also known as the Heated Nebulizer source) for the Q Trap and API LC/MS/MS systems. A more detailed and thorough account of these procedures can be found in the Q-exactive Operating Manual. The Q Exactive HF system combines a state-of-the-art segmented quadrupole for high-performance precursor ion selection with a high-resolution, accurate-mass (HR/AM) ultra-high-field Orbitrap mass analyzer to deliver a superior combination of scan speed, resolving power, mass accuracy, spectral quality and sensitivity. Log in your “Mass Spec Q-exactive” session on the CORES. Q Exactive Plus mass spectrometer. Exactive Series Installation Request Form Please refer to the Exactive Series Prei nstallation Requirements Guide (P/N 1288110, Re vision A) for the complete site requirem ents.
Perform routine identification, quantitation and confirmation in a single analysis with easy to use Thermo Scientific™ TraceFinder™acquisition and processing software. Which will be better for our task? This Exactive Operating Manualis intended for all personnel that need a thorough understanding of the instrument (to perform maintenance or troubleshooting, for example). Operating Manual: Exactive Series Software Manual: Exactive Plus. ITQ Manuals - English. The Thermo Scientific TM Q Exactive TM hybrid quadrupole-Orbitrap mass spectrometer introduced the revolutionary concept of Quanfirmation TM: the ability to routinely and confidently identify, quantify, and confirm in a single analysis using a single mass spectrometer. This manual should be kept near the instrument to be available for quick q exactive focus operating manual reference.
This Exactive Series Operating Manual represents the Original Operating Instructions. The Structure of Q Exactive Hybrid Quadrupole-Orbitrap Mass Spectrometer As shown in Figure 2, the Q Exactive hybrid quadrupole-Orbitrap mass spectrometer mainly includes an ion source, a stacked-ring ion guide (S-lens), a quadrupole mass filter, a curved linear trap (C-trap), a Higher Energy Collisional Dissociation (HCD) cell, and an Orbitrap. Q Exactive Focus Hybrid Quadrupole Orbitrap Mass Spectrometer Support › Q Exactive. Q Exactive Resolution at m/z 200 "Free" injection time ms Approx.
Exactive Series Software You can use the instrument control software to collect high-quality mass spectrometry data on the Thermo Scientific mass spectrometers. Scope of This Guide This manual includes the following chapters:. 7 Build 2659 were used to generate instrumental methods as well as to operate the mass spectrometer. In addition to this manual, Thermo Fisher Scientific provides other documents for the Exactive Plus mass spectrometer that are not part of the Original Operating Instructions. A new acquisition mode, Variable Data Independent Analysis.
For information about the operating procedures for the Exactive mass spectrometer, we recommend that you read the Exactive Operating Manual in its entirety. • The data system computer with the Q Exactive Tune software is switched on and the mass spectrometer is placed in Standby mode. The Exactive Family • The Exactive Plus • HCD cell optional • Upgradeable to Q Exactive • Mass range to m/z 6000 • Faster polarity switching • Rotated flatapole • New scan modes • The Q Exactive • Resolving power >140,000 • Parent ion selection capability • Spectral multiplexing • UHPLC and nanoflow capable. HRAM MS/MS for analytical confidence The Q Exactive Focus system can perform data-dependent “top 2 MS/MS” to generate spectra confirming analyte identification. This Exactive Software Manualprovides reference information about the parameters in the Instrument Configuration window, the Instrument Setup window, and the Exactive Tune window. This Exactive Series Operating Manual represents the Original Operating Instructions. Accelerated Higher Energy Collisional.
The Q Exactive HF-X MS provides best-in-class performance in peptides, proteins, and small molecule applications. AI/AS 1310 User Manuals AI/AS 3000 User Manuals TriPlus RSH User Manuals TriPlus 100 LS User Manuals TriPlus 300 Headspace User Manuals TriPlus Classic User Manuals TRACE 1300 Series GC User Manuals ISQ Series Manuals TSQ Series Manuals Legacy MS Manuals. The issues were apparently minor but the.
Workflow Advanced autosampler and liquid handling system improves lab productivity Laboratories can now automate manual steps and achieve high sample throughput and high productivity with a new autosampler and liquid handling system intended for use in pharmaceutical, contract research, food safety, environmental, clinical research and forensic workflows. The Q Exactive Focus is designed to deliver up to 70,000 resolution at m/z 200, and scan speed up to 12 Hz. The spectrometer is 2 years old. For information about performing these tasks, refer to the Exactive Series Operating Manual, the QExactiveHF Software Manualor the Q Exactive HF Tune Help, and the Ion Max and Ion Max-S API Source Hardware Manual. • Operating environment must be 15–26 °C (59–78 °F) and relative humidity must be 40–70% with no condensation Weight • Q Exactive Focus mass spectrometer: 182 kg (400 lbs) without forevacuum pump • Forevacuum pump: 62 kg (136 lbs) Dimensions • Q Exactive Focus mass spectrometer: (h × d × w) 95 × 83 × 91 cm (37 × 33 × 36 in.
Thermo persuades me to Q Exactive Focus Orbitrap LC-MS. Reference documentation for the Exactive Plus mass spectrometer includes the following:. Narrative: Ihor Batruch. I am currently working with a Q-Exactive Focus from Thermo and within 3 month, 2 electronic cards had to be replaced.
Getting Ions from Infusion Experiments. To view product manuals 1. Reference documentation for Exactive Series mass spectrometers includes the following:. This text is a guide to operating the Q-exactive mass spectroscopy. Thus, it is mandatory to read also the Exactive Series Operating Manual and the Ion Max and Ion Max-S API Source Hardware. Please note that this guide does q exactive focus operating manual not contain any safe ty notices and precautionary statements. Incredible resolving power up to 120,000 FWHM for the Q Exactive GC at m/z 200 and up to 50,000 FWHM for the Exactive GC at m/z 272, sub-ppm mass accuracy with a high acquisition rate, driving unrivaled spectral quality. The sensitivity, selectivity, flexibility, and ease-of-use provided by hybrid quadrupole-Orbitrap mass spectrometers set the standard for screening, quantitation, identification, and confirmation of targeted and untargeted compounds.
Qtof have 40,000. In this section, you can test whether the MS detector is operating properly. The high-resolution, accurate-mass Thermo Scientific™ Q Exactive™ Focus Hybrid Quadrupole-Orbitrap™ mass spectrometer allows for efficient screening, identification, confirmation, and quantitation of untargeted and targeted compounds for total confidence in authenticity. The Q Exactive focus HF-X MS takes identifi cation and quantitation to an unmatched level, making it possible to identify, quantify, and confi rm in a single analysis with a single instrument. I am a bit confused. The Q Exactive Focus mass spectrometer combines quadrupole precursor selection with high-resolution, accurate-mass detection to produce sensitivity that rivals triple quadrupole mass spectrometers and resolution that surpasses Q-TOF instruments.
This Q Exactive HF Software Manual provides reference information about the parameters in the Instrument Configuration window, the Instrument Setup window, and the Q Exactive HF Tune window. TSQ 8000 Evo Manuals - q exactive focus operating manual Spanish. Accelerated Higher Energy Collisional The system was operated either in the DDA mode or in the DIA mode.
Sub ppm mass accuracy has been achieved routinely in company and early access user. 13 and Tune version 2. From the Microsoft™ Windows™ taskbar, choose Start > Programs > Thermo Instruments > LTQ > Manuals > model.
Xcalibur version 4. Refer to the Q Exactive Operating Manualfor instructions about preparing the positive ion mode calibration solution or buying the ready-to-use solution from Thermo Fisher Scientific (product number 88323). In addition to this manual, Thermo Fisher Scientific provides other documents for Exactive Series mass spectrometers that are not part of the Original Operating Instructions. Q Exactive™ Focus Hybrid Quadrupole-Orbitrap Mass Spectrometer. Operating Manual: Exactive Series Specifications Sheet: Q Exactive Benchtop Quadrupole-Orbitrap Mass Spectrometer Search our database for Product Documents: Product Literature. • Velos Pro manual set You can access PDF files of the docume nts listed above an d of this guide from the data system computer. The Food and Drug Administration (FDA) released a liquid chromatography-high resolution mass spectrometry (LC-HRMS) method for the quantitation of N-nitrosodimethylamine (NDMA) in Ranitidine drug substance and drug products using the Q Exactive hybrid quadrupole-Orbitrap mass spectrometer.
Click the PDF file that you want to view. Thanks to its Orbitrap™ mass analyzer, the Exactive Plus. Infuse a low concentration calibration solution for positive ion mode – containing caffeine, MRFA, and Ultramark 1621 – into the ESI source using the syringe pump.
scan speed Hz/. For information about the operating proc edures for the Q Exactive HF mass spectrometer, we recommend that you read the Exactive Series Operating. This Exactive Plus Operating Manual represents the Original Operating Instructions.
Mass spectrometric detection was carried out on a Q Exactive HF orbitrap mass analyzer (Thermo Scientific, San Jose, CA, USA). scan speed Hz Resolution at m/z 200 "Free" injection time ms Approx. The software also provides Help. The Thermo q exactive focus operating manual Scientific Exactive Plus Orbitrap MS is a benchtop LC-MS system designed for high-performance, high-throughput screening, compound identification, and quantitative analysis.
See the Exactive Operating Manual for information about calibration solutions. Thermo Scientific™ TSQ™ triple. Q-exactive Mass spectrometer. The Q Exactive Focus mass spectrometer delivers qualitative and quantitative results every day. Control of the instruments is through two application packages: Tune and Method Editor.
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